Structures by: Block E.

Total: 41

5-endo-6-exo-bis(chloromethanesulfonyl)bicyclo[2.2.1]hept-2-ene

C7H8(SO2CH2Cl)2

Block, EricJeon, Hak RimZhang, Shao-ZhongDikarev, Evgeny V.

Organic letters (2004) 6, 3 437-440

a=9.9279(6)Å   b=7.8341(4)Å   c=15.8873(9)Å

α=90.00°   β=95.946(1)°   γ=90.00°

Dimethyl selenoxide

C2H6OSe

Filatov, Alexander S.Block, EricPetrukhina, Marina A.

Acta Crystallographica Section C (2005) 61, 10 o596-o598

a=4.9794(7)Å   b=6.1470(9)Å   c=6.8905(10)Å

α=106.850(2)°   β=90.177(2)°   γ=94.213(2)°

5-Thioniatelluroniabicyclo[3.3.0]octane bis(trifluoromethanesulfonate)

Te(CH2)6S(O3SCF3)2

Dennis H. EvansNadine E. GruhnJin JinBo LiEdward LoranceNoriko OkumuraNorma A. Macías-RuvalcabaUzma I. ZakaiShao-Zhong ZhangEric BlockRichard S. Glass

Journal of Organic Chemistry (2010) 75, 1997-2009

a=10.5080(4)Å   b=10.2087(4)Å   c=16.4276(7)Å

α=90.00°   β=103.5000(10)°   γ=90.00°

5-Thiatellurocane 5-Oxytris(pentafluorophenyl)boron

(Te(CH2)6S)OB(C6F5)3

Dennis H. EvansNadine E. GruhnJin JinBo LiEdward LoranceNoriko OkumuraNorma A. Macías-RuvalcabaUzma I. ZakaiShao-Zhong ZhangEric BlockRichard S. Glass

Journal of Organic Chemistry (2010) 75, 1997-2009

a=12.5426(6)Å   b=20.8109(9)Å   c=9.6271(4)Å

α=90.00°   β=95.7100(10)°   γ=90.00°

1,1'-Bis-5-thio-1-selenocanium Bis(B-hydroxy-tris[pentafluorophenyl)boron

[(Se(CH2)6S)2((C6F5)3BOH)2]((C6F5)3BOH2)2

Dennis H. EvansNadine E. GruhnJin JinBo LiEdward LoranceNoriko OkumuraNorma A. Macías-RuvalcabaUzma I. ZakaiShao-Zhong ZhangEric BlockRichard S. Glass

Journal of Organic Chemistry (2010) 75, 1997-2009

a=12.5471(7)Å   b=12.9889(7)Å   c=14.0208(7)Å

α=104.8930(10)°   β=93.1830(10)°   γ=93.9430(10)°

5,5'-Oxy-bis(5-thiatellurocane) Bis(tetrafluoroborate

(Te(CH2)6S)2O1(BF4)2

Dennis H. EvansNadine E. GruhnJin JinBo LiEdward LoranceNoriko OkumuraNorma A. Macías-RuvalcabaUzma I. ZakaiShao-Zhong ZhangEric BlockRichard S. Glass

Journal of Organic Chemistry (2010) 75, 1997-2009

a=9.5331(8)Å   b=9.0124(8)Å   c=13.0975(11)Å

α=90.00°   β=109.4920(10)°   γ=90.00°

Catena-((3,3-bis-methyl-1,3-selenasiletane) -dirhodium(ii)-tetratrifluoroacetate)

Rh2(O2CCF3)4Se(CH2)2Si(CH3)2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=9.5735(7)Å   b=11.3637(8)Å   c=13.0078(9)Å

α=65.7790(10)°   β=73.4060(10)°   γ=80.7200(10)°

3,3,7,7-Tetramethyl-1,5-dithia-3,7-disilocane

S2(CH2)4(Si(CH3)2)2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=6.6704(5)Å   b=9.8045(7)Å   c=10.8940(7)Å

α=98.9700(10)°   β=95.8430(10)°   γ=106.3500(10)°

5,5-Bis-trimethylsilyl-1,3,5-dithiasiletane

Si(Si(CH3)3)2(CH2)3S2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=13.8814(8)Å   b=9.1545(5)Å   c=12.5777(7)Å

α=90.00°   β=93.0450(10)°   γ=90.00°

3,3,4,4,8,8,9,9-Octamethyl-1,6-dithia-3,4,8,9-tetrasilacyclodecane

S2(CH2)4(Si(CH3)2)4

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=6.2586(4)Å   b=7.9795(5)Å   c=11.3208(7)Å

α=104.2230(10)°   β=93.6240(10)°   γ=107.7620(10)°

3,3,7,7-Tetramethyl-1,5-diselena-3,7-disilocane

Se2(CH2)4(Si(CH3)2)2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=7.3665(4)Å   b=13.2789(7)Å   c=14.1387(7)Å

α=90.00°   β=99.6510(10)°   γ=90.00°

3,3,4,4,8,8,9,9-Octamethyl-1,6-diselena-3,4,8,9-tetrasilacyclodecane

Se2(CH2)4(Si(CH3)2)4

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=6.2293(4)Å   b=8.0571(5)Å   c=11.4887(7)Å

α=103.8910(10)°   β=94.1820(10)°   γ=107.2310(10)°

3,3,7,7-Tetramethyl-1,5-diselena-3,7-distannocane

Se2(CH2)4(Sn(CH3)2)2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=9.097(2)Å   b=11.189(3)Å   c=7.0389(16)Å

α=90.00°   β=91.984(3)°   γ=90.00°

3,3-Bis-trimethylsilyl-1,3-selenasiletane

Se(CH2)2Si(Si(CH3)3)2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=12.2465(7)Å   b=12.1821(7)Å   c=9.7334(6)Å

α=90.00°   β=90.00°   γ=90.00°

1,3-thiaselenetane-1-oxide

Se(CH2)2SO

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=8.1944(5)Å   b=8.2657(5)Å   c=12.9537(9)Å

α=90.00°   β=90.00°   γ=90.00°

1,3-thiaselenetane-1,1-dioxide

Se(CH2)2SO2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=5.6201(6)Å   b=5.4290(6)Å   c=7.9280(9)Å

α=90.00°   β=101.007(2)°   γ=90.00°

3,3,7,7-Tetramethyl-3,7-disila-1,5-ditelluracyclooctane

Te2(CH2)4(Si(CH3)2)2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=8.0944(4)Å   b=25.8749(13)Å   c=10.6969(5)Å

α=90.00°   β=106.5830(10)°   γ=90.00°

3,3,7,7-tetrakis(trimethylsilyl)-3,7-disila-1,5-ditelluracyclooctane

Te2(CH2)4(Si(Si(CH3)3)2)2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=6.5427(3)Å   b=13.7608(6)Å   c=16.9840(8)Å

α=90.00°   β=98.6130(10)°   γ=90.00°

Bis(bromomethyl)bis(trimethylsilyl)silane

Si(CH2Br)2(Si(CH3)3)2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=17.4033(14)Å   b=7.8526(7)Å   c=12.3918(10)Å

α=90.00°   β=108.5570(10)°   γ=90.00°

1,1-Diiodo-3,3,4,4-tetramethyl-1,3,4-telluradisilolane

TeI2(CH2)2(Si(CH3)2)2

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=19.4457(8)Å   b=19.4457(8)Å   c=7.9176(6)Å

α=90.00°   β=90.00°   γ=90.00°

3,3-Bis-trimethylsilyl-1,3-thiasiletane

S(CH2)2Si(Si(CH3)3)2)

Eric BlockEvgeny V. DikarevRichard S. GlassJin JinBo LiXiaojie LiShao-Zhong Zhang

Journal of the American Chemical Society (2006) 128, 14949-14961

a=12.2325(11)Å   b=12.3562(11)Å   c=9.6165(9)Å

α=90.00°   β=90.00°   γ=90.00°

2,6-dithiaspiro[3.3]heptane

S2C5H8

Marina A. PetrukhinaColin HenckBo LiEric BlockJin JinShao-Zhong ZhangRodolphe Clerac

Inorganic Chemistry (2005) 44, 77-84

a=5.8013(4)Å   b=19.2532(12)Å   c=5.8183(4)Å

α=90.00°   β=109.7090(10)°   γ=90.00°

Catena-(bis(hexafluoroacetylacetonato)-nickel(II) -(mu2-2,6-diselenaspiro[3,3]heptane-Se,Se'))

[Ni(C5O2F6H)2(Se2C5H8)]

Marina A. PetrukhinaColin HenckBo LiEric BlockJin JinShao-Zhong ZhangRodolphe Clerac

Inorganic Chemistry (2005) 44, 77-84

a=7.5479(10)Å   b=18.739(3)Å   c=15.885(2)Å

α=90.00°   β=90.667(2)°   γ=90.00°

2-thia-6-selenaspiro[3.3]heptane

SSeC5H8

Marina A. PetrukhinaColin HenckBo LiEric BlockJin JinShao-Zhong ZhangRodolphe Clerac

Inorganic Chemistry (2005) 44, 77-84

a=5.8538(5)Å   b=19.4846(18)Å   c=5.8579(5)Å

α=90.00°   β=109.1230(10)°   γ=90.00°

Bis(hexafluoroacetylacetonato)-cobalt(II) dihydrate

[(Co(C5O2F6H)2)(OH2)2]

Marina A. PetrukhinaColin HenckBo LiEric BlockJin JinShao-Zhong ZhangRodolphe Clerac

Inorganic Chemistry (2005) 44, 77-84

a=21.2490(12)Å   b=8.0736(4)Å   c=9.6680(5)Å

α=90.00°   β=95.4830(10)°   γ=90.00°

Tris(bis(hexafluoroacetylacetonato)-copper(II)) -bis(mu2-2,6-diselenaspiro[3,3]heptane-Se, Se')

[(Cu(C5O2F6H)2)3(Se2C5H8)2]

Marina A. PetrukhinaColin HenckBo LiEric BlockJin JinShao-Zhong ZhangRodolphe Clerac

Inorganic Chemistry (2005) 44, 77-84

a=11.1179(9)Å   b=11.5052(10)Å   c=12.3911(11)Å

α=90.6540(10)°   β=99.2800(10)°   γ=110.5090(10)°

Tris(bis(hexafluoroacetylacetonato)-copper(II)) -bis(mu2-2-thia-6-selenaspiro[3,3]heptane-Se,S)

[(Cu(C5O2F6H)2)3(SSeC5H8)2]

Marina A. PetrukhinaColin HenckBo LiEric BlockJin JinShao-Zhong ZhangRodolphe Clerac

Inorganic Chemistry (2005) 44, 77-84

a=11.2238(15)Å   b=11.4147(15)Å   c=12.4732(17)Å

α=91.251(2)°   β=98.773(2)°   γ=110.096(2)°

Catena-(bis(hexafluoroacetylacetonato)-cobalt(II) -(mu2-2,6-diselenaspiro[3,3]heptane-Se,Se'))

[Co(C5O2F6H)2(Se2C5H8)]

Marina A. PetrukhinaColin HenckBo LiEric BlockJin JinShao-Zhong ZhangRodolphe Clerac

Inorganic Chemistry (2005) 44, 77-84

a=7.5777(9)Å   b=18.924(2)Å   c=15.8309(18)Å

α=90.00°   β=91.527(2)°   γ=90.00°

Diselenadispiroheptane

Se(CH2)2C(CH2)2Se

Evgeny V. DikarevRoman V. ShpanchenkoKristian W. AndreiniEric BlockJin JinMarina A. Petrukhina

Inorganic Chemistry (2004) 43, 5558-5563

a=5.9123(4)Å   b=19.6400(13)Å   c=5.8877(4)Å

α=90.00°   β=108.5500(10)°   γ=90.00°

Rhodium acetate

Rh2(O2CCH3)4

Evgeny V. DikarevRoman V. ShpanchenkoKristian W. AndreiniEric BlockJin JinMarina A. Petrukhina

Inorganic Chemistry (2004) 43, 5558-5563

a=8.3392(7)Å   b=5.2216(5)Å   c=7.5264(6)Å

α=96.547(10)°   β=78.101(6)°   γ=104.714(13)°

Catena(mu-2.6-diselenaspiro[3.3]heptane-Se,Se') tetrakis(mu-acetato-O,O')-dirhodium(II,II))

Rh2(O2CCH3)4(Se(CH2)2C(CH2)2Se)

Evgeny V. DikarevRoman V. ShpanchenkoKristian W. AndreiniEric BlockJin JinMarina A. Petrukhina

Inorganic Chemistry (2004) 43, 5558-5563

a=8.1357(4)Å   b=8.7736(4)Å   c=15.2183(8)Å

α=77.4170(30)°   β=88.8369(26)°   γ=69.276(4)°

Catena-{tetrakis(trifluoroacetato)dirhodium(II,II)- -(μ2-dimethylselenide)}

[Rh2(O2C2F3)4(Se(CH3)2)]

Evgeny V. DikarevMarina A. PetrukhinaXiaojie LiEric Block

Inorganic Chemistry (2003) 42, 1966-1972

a=13.736(5)Å   b=8.522(5)Å   c=18.085(2)Å

α=90.00°   β=91.09(2)°   γ=90.00°

Tetrakis(trifluoroacetato)dirhodium(II,II)-bis (ν1-dimethylselenoxide,-O)

[Rh2(O2C2F3)4]((CH3)2SeO)2

Evgeny V. DikarevMarina A. PetrukhinaXiaojie LiEric Block

Inorganic Chemistry (2003) 42, 1966-1972

a=8.5443(9)Å   b=9.761(3)Å   c=14.603(3)Å

α=84.477(3)°   β=88.52(1)°   γ=87.51(1)°

Catena-{tetrakis(trifluoroacetato)dirhodium(II,II)-(μ2- dimethylselenoxide,-O)},benzene solvate

[Rh2(O2C2F3)4((CH3)2SeO)],1/2C6H6

Evgeny V. DikarevMarina A. PetrukhinaXiaojie LiEric Block

Inorganic Chemistry (2003) 42, 1966-1972

a=11.288(1)Å   b=11.8657(9)Å   c=20.040(1)Å

α=74.657(6)°   β=81.996(6)°   γ=64.516(4)°

Catena-{tetrakis(mu2-trifluoroacetato-O,O')-(mu2-diphenyl selenone-O,O')]- di-rhodium(II,II)},1,2-dichloroethane solvate

[Rh2(O2CCF3)4((C6H5)2SeO2)],(C2H4Cl2)

Evgeny V. DikarevRenee Y. BeckerEric BlockZhixing ShanR. Curtis HaltiwangerMarina A. Petrukhina

Inorganic Chemistry (2003) 42, 7098-7105

a=11.8427(7)Å   b=12.9521(8)Å   c=13.2926(8)Å

α=108.9900(10)°   β=97.7230(10)°   γ=117.0250(10)°

Catena-(tetrakis(mu2-trifluoroacetateo-O,O')-(mu2-dimethyl sulfone-O,O') -di-rhodium(II,II))

[Rh2(O2CCF3)4((CH3)2SO2)]

Evgeny V. DikarevRenee Y. BeckerEric BlockZhixing ShanR. Curtis HaltiwangerMarina A. Petrukhina

Inorganic Chemistry (2003) 42, 7098-7105

a=9.062(2)Å   b=9.681(1)Å   c=13.244(2)Å

α=103.70(2)°   β=102.63(2)°   γ=106.55(1)°

Catena-(tetrakis(mu2-trifluoroacetato-O,O')-(mu2-diphenyl sulfone-O,O') -di-rhodium(II,II))

[Rh2(O2CCF3)4((C6H5)2SO2)]

Evgeny V. DikarevRenee Y. BeckerEric BlockZhixing ShanR. Curtis HaltiwangerMarina A. Petrukhina

Inorganic Chemistry (2003) 42, 7098-7105

a=11.1098(9)Å   b=11.9417(9)Å   c=12.9680(9)Å

α=96.876(7)°   β=112.277(8)°   γ=110.450(4)°

Dimethyl selenone

(CH3)2SeO2

Evgeny V. DikarevRenee Y. BeckerEric BlockZhixing ShanR. Curtis HaltiwangerMarina A. Petrukhina

Inorganic Chemistry (2003) 42, 7098-7105

a=8.8118(9)Å   b=8.4480(9)Å   c=6.9904(7)Å

α=90.00°   β=120.184(2)°   γ=90.00°

Tetrakis(mu2-trifluoroacetato-O,O')-bis(diphenyl sulfone-O)-di-rhodium(II,II)), dichloromethane solvate

Rh2(O2CCF3)4[(C6H5)2SO2]2,2(CH2Cl2)

Evgeny V. DikarevRenee Y. BeckerEric BlockZhixing ShanR. Curtis HaltiwangerMarina A. Petrukhina

Inorganic Chemistry (2003) 42, 7098-7105

a=8.3668(7)Å   b=9.4711(8)Å   c=14.2118(12)Å

α=86.2260(10)°   β=73.8870(10)°   γ=88.1540(10)°

Tetrakis(mu2-trifluoroacetato-O,O')-bis(dimethyl selenone-O)- di-rhodium(II,II))

Rh2(O2CCF3)4((CH3)2SeO2)2

Evgeny V. DikarevRenee Y. BeckerEric BlockZhixing ShanR. Curtis HaltiwangerMarina A. Petrukhina

Inorganic Chemistry (2003) 42, 7098-7105

a=9.3124(9)Å   b=10.3370(18)Å   c=13.9739(19)Å

α=83.767(3)°   β=72.945(3)°   γ=80.511(3)°

Catena-(tetrakis(mu2-trifluoroacetato-O,O')-(mu2-diphenyl selenone-O,O')- di-rhodium(II,II))

Rh2(O2CCF3)4((C6H5)2SeO2)

Evgeny V. DikarevRenee Y. BeckerEric BlockZhixing ShanR. Curtis HaltiwangerMarina A. Petrukhina

Inorganic Chemistry (2003) 42, 7098-7105

a=10.1378(6)Å   b=20.4656(12)Å   c=13.1423(8)Å

α=90.00°   β=90.00°   γ=90.00°